All posts by Shulgin Ann & Alexander

  • 2C-T-9

        2,5-DIMETHOXY-4-(t)-BUTYLTHIOPHENETHYLAMINE SYNTHESIS: To a well-stirred ice-cold suspension of 2.8 g p-dimethoxybenzene and 3.2 mL N,N,N‘,N‘-tetramethylethylenediamine in 100 mL petroleum ether under an inert atmosphere...

  • 2C-T-8

        2,5-DIMETHOXY-4-CYCLOPROPYLMETHYLTHIOPHENETHYLAMINE SYNTHESIS: To a solution of 2.8 g of KOH pellets in 25 mL hot MeOH, there was added a mixture of 5.9 g...

  • 2C-T-7

        2,5-DIMETHOXY-4-(n)-PROPYLTHIOPHENETHYLAMINE SYNTHESIS: To a solution of 3.4 g of KOH pellets in 50 mL hot MeOH, there was added a mixture of 6.8 g...

  • psi-2C-T-4

        2,6-DIMETHOXY-4-(i)-PROPYLTHIOPHENETHYLAMINE) SYNTHESIS: A stirred solution of 8.3 g 3,5-dimethoxy-1-chlorobenzene and 7.2 g isopropylsulfide in 100 mL anhydrous Et2O was cooled with an external ice...

  • 2C-T-4

        2,5-DIMETHOXY-4-(i)-PROPYLTHIOPHENETHYLAMINE SYNTHESIS: To a solution of 2.5 g of KOH pellets in 40 mL hot EtOH, there was added 5.4 g 2,5-dimethoxythiophenol (see under 2C-T-2 for...

  • 2C-T-2

        2,5-DIMETHOXY-4-ETHYLTHIOPHENETHYLAMINE SYNTHESIS: To a solution of 165 g 1,4-dimethoxybenzene in 1 L of CH2Cl2, in a well ventilated place and well stirred, there was...

  • 2C-T

        2,5-DIMETHOXY-4-METHYLTHIOPHENETHYLAMINE SYNTHESIS: A solution of 149 g sodium thiosulfate in 300 mL H2O was vigorously stirred. To this there was added, over the course...

  • 2C-SE

        2,5-DIMETHOXY-4-METHYLSELENEOPHENETHYLAMINE SYNTHESIS: A suspension of 5.65 g 1,4-dimethoxybenzene in 100 mL petroleum ether containing 6.5 mL N,N,N‘,N‘-tetramethylethylenediamine was magnetically stirred, placed in an inert...

  • CPM

        CYCLOPROPYLMESCALINE; 4-CYCLOPROPYLMETHOXY-3,5-DIMETHOXYPHENETHYLAMINE SYNTHESIS: To a solution of 2.8 g homosyringonitrile (see under E for synthesis) in 20 ml acetone containing about 50 mg decyltriethylammonium...

  • 2C-P

        2,5-DIMETHOXY-4-(n)-PROPYLPHENETHYLAMINE SYNTHESIS: To a stirred solution of 138 g p-dimethoxybenzene in 400 mL CH2Cl2 there was added a suspension of 172 g anhydrous AlCl3...

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